主要特点
升华仪(有机小分子提纯设备)主要用途是在真空条件下对有机混合物进行升华达到纯化的目的(即蒸发后重结晶)，主要处理的对象为具有升华性的有机材料，或具有流动相特性混合物如有机声光产品(如有机发光显示器用的有机光电材料)或纳米材料。
贝意克提供满足从研发级，中试级直至产业化级别所需的多种规格的升华仪，有利于用户实现从实验室到生产线的无缝对接。
此类设备采用真空吸附球头挤压密封，结构简单，便于拆卸。方便进放物料，易于操作。
Sublimation instrument(Organic ***all Molecule Purification Equipment) is to purify the organic mixture under vacuum conditi*** ( re-crystallization after evaporation). The main treatment object is sublimable organic material, or a mixture with mobile phase characteristics such as organic sound and light products (such as An organic photoelectric material for an organic light emitting display) or a nano material.
BEQ provides a variety of sublimation instruments that meet the needs of R&D, pilot and industrialization levels, enabling users to seamlessly integrate from laboratory to production line.
Adopt Vacuum adsorption ball head extrusion seal.The structure is simple and easy to disassemble. Convenient to put in and put materials also operate.
技术参数Technical Parameters
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升华炉Sublimation furnace |
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功率Power |
5KW |
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电压Voltage |
AC220V 50/60Hz |
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加热元件heating element |
进口KTL电阻丝 resistance wire |
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加热区heating zone |
3区，3点***控温 three zones,three points temp. control independently |
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温区长度 length of zone |
200+300+200mm（可定制）(customizable) |
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升华区及保温区温度Sublimation area and insulation zone temperature |
室温至800℃，连续可调 Continuously adjustable from room temperature to 800 ° C |
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数字工控仪表与PLC双控，模糊型PID控制。 PID automatic and double control by digital industrial instrument and PLC
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无纸记录Paperless record |
内置存储记录运行工艺数据，外接USB接口，可以电脑连接一键拷贝数据。 Built-in storage record running process data, external USB interface, you can connect one-click copy data with computer. |
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结构描述Structure |
1）设备对半开启； half open 2）进料端配备高精度质量流量计，准确控制气体流量，可以实现生产工艺拓展和调整； The feeding end is equipped with a high-precision mass flow meter to accurately control the gas flow, which can realize the expansion and adjustment of the production process. 3）采用自动化工艺流程，设定好工艺一键操作。降低人为因素，工艺可靠性达到99.9%。 Automated process flow is used to set the process for one-button operation. Reduce human factors and achieve a process reliability of 99.9%.
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过滤方式Filter |
采用多级过滤保护装置，包括微孔金属滤网、液氮内嵌式冷凝阱。Multi-level filter protection device including Microporous metal filter ,condensation trap liquid nitrogen embedded |
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Pla***a系统Pla***a system |
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腔体chamber |
内外石英管装置，可保证真空室管不受污染，且易于清洗。 The inner and outer quartz tube devices ensure that the vacuum chamber tubes are free from contamination and are easy to clean.
内层料管分段升华后各段料容易区分，能***大限度的保证产品的纯度和产率。 After the inner layer tube is sublimated, the secti*** are easy to distinguish, which can ensure the purity and yield of the product to the utmost extent.
外管（单端封口）：60/100*1000mm，内管根据要求定制 Outer tube (single-end sealing): 60/100*1000mm, the inner tube is customized according to requirements |
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真空系统vacuum unit |
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采用主管和分子泵直连，确保实验中高真空要求，真空度可达10 -4Pa |
Direct connection with the main tube and molecular pump to ensure high vacuum in the experiment, the vacuum can reach 10 -4Pa |
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前级泵Fore pump |
抽速pumping speed：165L/Min |
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分子泵Molecular pump |
抽速pumping speed：49L/S（KF40接口） 转速Rotating speed：81000rpm |